HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54243338, compound → HCID 19004462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54243338 | HCID 54243338 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 19004462 | HCID 19004462 | 72.6% |
Reaction Steps
A mixture of 4-[(3-phenylpropyl)oxy]-alpha-oxobenzeneacetic acid methyl ester (0.65 g) in methanol and 0.5N sodium hydroxide (8 mL) was treated as in Example 19. Extraction provided 0.6 g which solidified and was crystallized from benzene-hexane to give 0.45 g of colorless 4-[(3-phenylpropyl)oxy]-alpha-oxobenzeneacetic acid, mp 58°-59° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-33c70746287b4c36ab0c6e7210f6f8e6 |
| Source note | uspto-grants-1994_09 |