HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67757615, compound → HCID 19004398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67757615 | HCID 67757615 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 19004398 | HCID 19004398 | — |
Reaction Steps
A mixture of (E)-alpha-oxo-4- [(3-phenyl-2-propenyl)oxy]benzeneacetic acid methyl ester 0. 1 molar hydrate (0.7 g) in methanol and 0.5N sodium hydroxide (8 mL) was treated as in Example 19. Extraction provided solids which were crystallized from diethyl etherhexane to give 0.55 g of colorless (E)-alpha-oxo-4-[(3-phenyl-2-propenyl)oxy]benzeneacetic acid, mp 111°-112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-c2bc2fa50b55408594704578115a5ed6 |
| Source note | uspto-grants-1994_09 |