HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53839912, compound → HCID 19004410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53839912 | HCID 53839912 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 19004410 | HCID 19004410 | 56.5% |
Reaction Steps
A mixture of alpha-oxo-4-[[(3-phenoxy)propyl]oxy]benzeneacetic acid methyl ester (0.63 g) in methanol and 0.5N sodium hydroxide (8 mL) was treated as in Example 19. Extraction with dichloromethane provided material which was crystallized from diethyl ether-hexane to give 0.34 g of colorless alpha-oxo-4-[[(3-phenoxy)propyl]oxy]benzeneacetic acid, mp 50°-52° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-a613818d8e2041e78498f21d7ce81c9d |
| Source note | uspto-grants-1994_09 |