HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53757285, compound → HCID 19004288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53757285 | HCID 53757285 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 19004288 | HCID 19004288 | 69.4% |
Reaction Steps
A mixture of alpha-oxo-4-[[(6-phenoxy)hexyl]oxy]benzeneacetic acid methyl ester (0.75 g) in methanol and 0.5N sodium hydroxide (8 mL) was treated as in Example 19. Extraction provided solids which were crystallized from diethyl ether-hexane to give 0.5 g of colorless alpha-oxo-4-[[(6-phenoxy)hexyl]oxy]benzeneacetic acid, mp 121°-122° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-bcf0c61b949f479d8949491a8662ae94 |
| Source note | uspto-grants-1994_09 |