HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53815443, compound → HCID 19004380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53815443 | HCID 53815443 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 19004380 | HCID 19004380 | 90% |
Reaction Steps
A mixture of alpha-oxo-4-[[2-(phenylthio)ethyl]oxy]benzeneacetic acid methyl ester (0.5 g) in methanol and 0.5N sodium hydroxide (6 mL) was treated as in Example 19. Extraction provided material which was crystallized from benzene-hexane to give 0.43 g of colorless alpha-oxo-4-[[2-(phenylthio)ethyl]oxy]benzeneacetic acid, mp 72°-73° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05344843 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-b44306ca21cb46fcbcbc94291813db52 |
| Source note | uspto-grants-1994_09 |