HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53783517, compound → HCID 18964404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53783517 | HCID 53783517 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18964404 | HCID 18964404 | — |
Reaction Steps
0.01 mol of 2,2,3,3-tetrafluoropropyl p-(5-heptyl-pyrimidin-2-yl)-cinnamate (for preparation see Example 21) are hydrogenated in THF with Pd/C in the known manner. Usual working-up gives 2,2,3,3-tetrafluoropropyl β-[p-(5-heptyl-pyrimidin-2-yl)-phenyl]-propionate of m.p. 42° and c.p. 54°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05348677 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-e1de1d26b85a41a2a7182354596ca6b2 |
| Source note | uspto-grants-1994_09 |