Cyanuric chloride → HCID 18965200, compound

HRID 2226379Notes

Reaction equation

HRID 2226379 reaction equation
N1C(Cl)=NC(Cl)=NC=1Cl.[Cl:10][C:11]1[N:16]=[C:15]([CH:17]2[CH2:20][CH2:19]C2)[N:14]=[C:13]([NH:21][CH:22]2[CH2:24][CH2:23]2)[N:12]=1>>[Cl:10][C:11]1[N:16]=[C:15]([CH:17]2[CH2:20][CH2:19]2)[N:14]=[C:13]([NH:21][CH:22]2[CH2:23][CH2:24]2)[N:12]=1

Participants

3

Reactant 2

HCID 7954Cyanuric chloride2×HCID 18965201HCID 18965201, compound

Product 1

HCID 18965200HCID 18965200, compound

Procedure

This compound is recrystallized from hexane. Yield (calculated on the basis of cyanuric chloride): 71.5%. M.P.: 66°-67° C. 2-Chloro-4-cyclobutyl-6-cyclopropylamino-1,3,5-triazine. Crude yield (calculated on the basis of the cyanuric chloride): 23%. The product is used as such, without other purification, in the following step.

Workup

  1. customThis compound is recrystallized from hexane
  2. customYield (
  3. customCrude yield (
  4. customwithout other purification

Sources & evidence

ORD record
ord-2177b77c39744d69972d2465fab631ff
Source dataset
uspto-grants-1994_09
Patent number
US05348956

Reaction notes

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