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HRID2226421

反应详情

EQUATION

反应方程式

HRID 2226421 的结构方程式

REACTANTS

反应物

1
结构：C[C@H](NC(=O)OCc1ccccc1)C(=O)N1C2COCC2C[C@H]1C(=O)O
HCID18654884

未命名化合物

PRODUCTS

生成物

1
结构：C[C@H](N)C(=O)N1C2COCC2C[C@H]1C(=O)O
HCID18654890

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Dissolve 1-[N-benzyloxycarbonyl-(S)-alanyl]hexhydrofuro[3,4-b]pyrrole-2(S)-carboxylic acid in methanol. Add 10% palladium-on-charcoal and hydrogenate the mixture at atmospheric pressure. Filter the mixture and concentrate in vacuo to give 1-[(S)-alanyl]hexahydrofuro[3,4-b]pyrrole-2(S)-carboxylic acid.

WORKUP

后处理

  1. filtrationFilter the mixture
  2. concentrationconcentrate in vacuo