HRID2226814

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID69144

Isopropyl phenyl ketone

C10H12O

结构：[N-]=[N+]=C(S(=O)(=O)C1CCCCC1)S(=O)(=O)C1CCCCC1

HCID11056751

BIS(CYCLOHEXYLSULFONYL)DIAZOMETHANE

C13H22N2O4S2

结构：Cc1ccc(S(=O)(=O)OCc2c([N+](=O)[O-])cccc2[N+](=O)[O-])cc1

HCID11175590

未命名化合物

PRODUCTS

生成物

结构：Cc1ccc(S(=O)(=O)C(C)(C)C(=O)c2ccccc2)cc1

HCID13445258

2-Methyl-2-(4-methylbenzene-1-sulfonyl)-1-phenylpropan-1-one

C17H18O3S

PROCEDURE

实验过程

Using isobutyrophenone, the reaction was carried out in the same manner as described in Synthesis Example 9, (2) and (3), the crude solid was recrystallized from methanol to afford 2-methyl-2-(p-toluenesulfonyl)propiophenone as a white needles.

WORKUP

后处理

customthe crude solid was recrystallized from methanol