HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18963816, compound → HCID 18963819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18963816 | HCID 18963816 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 18963819 | HCID 18963819 | 89% |
Reaction Steps
135 mg of 6-benzyloxy-4-methoxymethyl-β-carboline-3carboxylic acid-(2-phenyl-1,3-dioxan-5-yl)-ester under 10 ml of acetone and 100 ml of 4N hydrochloric acid is stirred for 1 hour at 80° C. bath temperature. The batch is concentrated by evaporation, taken up in aqueous ammonia and suctioned off. 100 mg of 6-benzyloxy-4-methoxymethyl-β-carboline-3-carboxylic acid-(1,3-dihydroxy-propan-2-yl)-ester of a melting point of 190°-192° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05350750 |
| Source dataset | uspto-grants-1994_09 |
| ORD ID | ord-ab1a5cad7c9f462db9c0e3ef74cd285c |
| Source note | uspto-grants-1994_09 |