HCID 15233845, compound → HCID 18963999, compound

Participants

Reaction Steps

In a 500 ml Parr hydrogenation bottle was suspended 0.5 g of 10% Pd/C in 50 ml of ethyl alcohol. To this was added a solution of 1,2,3,4-tetrahydro-7-phenylmethoxy-N,N,4-trimethylcyclopent[b]indole-2-methanamine (2.3 g, 0.007 mole) in 200 ml of ethyl alcohol. After shaking at 50° C. under 50 psi hydrogen for two hours, the mixture was cooled and filtered, and the filtrate concentrated to a tan solid, 1.5 g, m.p. 110° C.

Provenance & Evidence