HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → (4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | (4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)acetic acid | HCID 18471803 | — |
| Product | (4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)acetyl chloride | HCID 18471799 | — |
Reaction Steps
To a 100 mL flask containing a stirbar is added the acid 2B (R=4-Methyl-3-pentenyl) (10 g) and oxalyl chloride (8.3 mL). The reaction is stirred under a nitrogen atmosphere for one hour after gas evolution ceases. Residual oxalyl chloride is removed in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06413448B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-f7a2900f3ceb4afbb7ca027c24dcc3cd |
| Source note | uspto-grants-2002_07 |