反应详情

To a 100 mL flask containing a stirbar is added the acid 2B (R=4-Methyl-3-pentenyl) (10 g) and oxalyl chloride (8.3 mL). The reaction is stirred under a nitrogen atmosphere for one hour after gas evolution ceases. Residual oxalyl chloride is removed in vacuo.

1. additionTo a 100 mL flask containing a stirbar
2. customResidual oxalyl chloride is removed in vacuo