HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylethanol → HCID 18471977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylethanol | HCID 6054 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Styrene-4-sulfonyl chloride | HCID 9855777 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18471977 | HCID 18471977 | — |
Reaction Steps
2-Phenylethanol (3.1 g) was reacted with p-styrene sulfonyl chloride (5.3 g) and triethylamine (2.7 g) in 20 ml of dichloromethane for 3 hours to give the desired product as a light yellow viscous oil that was purified by passing through basic aluminum oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06413694B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-874be716e65d480aa5a1a5e256a07d9a |
| Source note | uspto-grants-2002_07 |