HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70158897, compound → HCID 70159230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70158897 | HCID 70158897 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70159230 | HCID 70159230 | — |
Reaction Steps
To stirred solution of 4-6 (250 mg) in methanol (15 mL) was added a suspension of 10% Pd on carbon (90 mg) in ethanol (2 mL). The resulting suspension was stirred under an atmosphere of hydrogen for 1.5 hours. The mixture was filtered through Celite. The solvent was evaporated to give 4-7 as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06413955B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-705f7ff7e219400495cd826badf36164 |
| Source note | uspto-grants-2002_07 |