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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2227284Generated: October 30, 2026

HCID 70159372, compound → HCID 70159444, compound

https://huagongshe.com/reaction/2227284

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 70159372HCID 70159372—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
SolventMethanolHCID 887—
ProductHCID 70159444HCID 70159444—

Reaction Steps

To stirred solution of 5-3 (180 mg) in methanol (8 mL) was added a suspension of 10% Pd on carbon (60 mg) in ethanol (1 mL). The resulting suspension was stirred under an atmosphere of hydrogen for 1.5 hours. The mixture was filtered through Celite. The solvent was evaporated to give 5-4 as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06413955B1
Source datasetuspto-grants-2002_07
ORD IDord-666cbf38453744b6ba9f5634eeb712fd
Source noteuspto-grants-2002_07