HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70159372, compound → HCID 70159444, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70159372 | HCID 70159372 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 70159444 | HCID 70159444 | — |
Reaction Steps
To stirred solution of 5-3 (180 mg) in methanol (8 mL) was added a suspension of 10% Pd on carbon (60 mg) in ethanol (1 mL). The resulting suspension was stirred under an atmosphere of hydrogen for 1.5 hours. The mixture was filtered through Celite. The solvent was evaporated to give 5-4 as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06413955B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-666cbf38453744b6ba9f5634eeb712fd |
| Source note | uspto-grants-2002_07 |