HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178478732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Iodobenzylamine hydrochloride | HCID 2723861 | — |
| Reactant | 2,6-dichloro-9-cyclopentyl-9H-purine | HCID 10801116 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178478732 | HCID 178478732 | 93.3% |
Reaction Steps
Dissolve 2,6-dichloro-9-cyclopentylpurine (620 mg, crude), 3-iodobenzylamine hydrochloride (810 mg, 3.00 mmol) and triethylamine (835 μL, 6.00 mmol) in dry ethanol (20 mL). Heat at reflux for 15 hours, cool, and filter the solid to give the title compound as a white solid (680 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06413974B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-eaa48226350e4cfc8519326fc290f9a6 |
| Source note | uspto-grants-2002_07 |