2,4-Dichlorobenzylamine → HCID 18473341, compound

HRID 2227332Notes

Reaction equation

HRID 2227332 reaction equation
[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4](Cl)[N:3]=1.[Cl:17][C:18]1[CH:25]=[C:24]([Cl:26])[CH:23]=[CH:22][C:19]=1[CH2:20][NH2:21]>C(N(CC)CC)C>[Cl:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[C:4]([NH:21][CH2:20][C:19]2[CH:22]=[CH:23][C:24]([Cl:26])=[CH:25][C:18]=2[Cl:17])[N:3]=1

Participants

4

Reactant 2

HCID 14852,4-DichlorobenzylamineHCID 108011162,6-dichloro-9-cyclopentyl-9H-purine

Product 1

HCID 18473341HCID 18473341, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

2-Chloro-6-[(2,4-dichlorobenzyl)amino]-9-cyclopentylpurine is prepared from 2,6-dichloro-9-cyclopentylpurine, 2,4-dichlorobenzylamine, and triethylamine essentially as described above in Example 1, Scheme A, step b.

Sources & evidence

ORD record
ord-4f279a6312b94633b6c0b5dd1dd36db8
Source dataset
uspto-grants-2002_07
Patent number
US06413974B1

Reaction notes

Loading…