HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 2-(1-Benzylpiperidin-2-yl)ethan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Piperidin-2-ylethanol | HCID 15144 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 2-(1-Benzylpiperidin-2-yl)ethan-1-ol | HCID 10242551 | 100% |
Reaction Steps
2-Piperidineethanol (25.8 g, 0.2 mol), benzyl bromide (26.2 ml) and potassium carbonate (55.3 g) in acetonitrile (250 ml), as described above, gave 1-benzyl-2-piperidineethanol (43.8 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06413987B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-0799a95b340b4e9f9dd17761909f0657 |
| Source note | uspto-grants-2002_07 |