Hydrochloric Acid → HCID 178477480, compound

HRID 2227473Notes

Reaction equation

HRID 2227473 reaction equation
C(OC([N:8]([CH2:16][C:17]1[CH:18]=[C:19]([NH:28][C:29](=[NH:33])[S:30][CH2:31][CH3:32])[CH:20]=[CH:21][C:22]=1[N:23]1[CH:27]=[CH:26][CH:25]=[CH:24]1)C(OC(C)(C)C)=O)=O)(C)(C)C.[ClH:34]>>[ClH:34].[ClH:34].[NH2:8][CH2:16][C:17]1[CH:18]=[C:19]([NH:28][C:29](=[NH:33])[S:30][CH2:31][CH3:32])[CH:20]=[CH:21][C:22]=1[N:23]1[CH:24]=[CH:25][CH:26]=[CH:27]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178477481HCID 178477481, compound

Product 1

HCID 178477480HCID 178477480, compoundYield 96%

Procedure

A mixture of the compound (40 mg) obtained in Example 1g and 4 N HCl (10 ml) was stirred at room temperature for 1 hour and then concentrated at reduced pressure to give the titled compound (28 mg; yield, 96%).

Workup

  1. concentrationconcentrated at reduced pressure

Sources & evidence

ORD record
ord-5201f1e03ce74f7c9d30e9392a83d6b9
Source dataset
uspto-grants-2002_07
Patent number
US06414005B1

Reaction notes

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