HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 178468350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 54233451 | HCID 54233451 | — |
| Product | HCID 178468350 | HCID 178468350 | 61% |
Reaction Steps
A mixture of the compound (243 mg) obtained in Example 4a and saturated HCl-ethanol (10 ml) was stirred at room temperature for 29 hours. The reaction mixture was concentrated at reduced pressure and the resulting residue was recrystallized from ethanol-ethyl acetate to give the titled compound (yield, 61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06414005B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-b872c31624a8441395b64f4080b8892c |
| Source note | uspto-grants-2002_07 |