Hydrochloric Acid → HCID 178477482, compound

HRID 2227483Notes

Reaction equation

HRID 2227483 reaction equation
C(OC([NH:8][CH2:9][C:10]1[C:11]([CH3:27])=[C:12]([NH:21][C:22](=[NH:26])[S:23][CH2:24][CH3:25])[CH:13]=[CH:14][C:15]=1[N:16]1[CH:20]=[CH:19][CH:18]=[N:17]1)=O)(C)(C)C.[ClH:28]>>[ClH:28].[ClH:28].[NH2:8][CH2:9][C:10]1[C:11]([CH3:27])=[C:12]([NH:21][C:22](=[NH:26])[S:23][CH2:24][CH3:25])[CH:13]=[CH:14][C:15]=1[N:16]1[CH:20]=[CH:19][CH:18]=[N:17]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 178477483HCID 178477483, compound

Product 1

HCID 178477482HCID 178477482, compoundYield 93%

Procedure

A mixture of the compound (47 mg) obtained in Example 7f and 6 N HCl (6 ml) was stirred at room temperature for 3 hours. The reaction mixture was concentrated at reduced pressure to give the titled compound (yield, 93%).

Workup

  1. concentrationThe reaction mixture was concentrated at reduced pressure

Sources & evidence

ORD record
ord-a34e31bc4a40455caf285cb03fef4e18
Source dataset
uspto-grants-2002_07
Patent number
US06414005B1

Reaction notes

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