HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → HCID 9937045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18474327 | HCID 18474327 | — |
| Product | HCID 9937045 | HCID 9937045 | — |
Reaction Steps
The preparation was carried out analogously to Example 1 using 5-[2-(5-tert-butyl-2-methoxybenzamido)ethyl]-2-(2-methoxyethoxy)benzenesulfonamide. Instead of potassium carbonate, sodium hydride was used as base in the reaction with methyl isothiocyanate analogously to Example 5. The product had a melting point of 61° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06414030B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-9d51e3325afc4582abd28e68f24adebd |
| Source note | uspto-grants-2002_07 |