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HRID222770

反应详情

EQUATION

反应方程式

HRID 222770 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N1CCc2ccc(B(O)O)cc2CC1
HCID57440296

3-(1,1-Dimethylethyl) 7-borono-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate

C15H22BNO4

结构：CNC(=O)c1ccc(Oc2ccc3c(c2)CCN(C2CCC2)CC3)c(C#N)c1
HCID57440313

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)c1ccc(Oc2ccc3c(c2)CCN(C(=O)OC(C)(C)C)CC3)c(C#N)c1
HCID68508039

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 3-cyano-4-hydroxy-N-methylbenzamide (E279, Step 3) and (3-{[(1,1-dimethylethyl)oxy]carbonyl}-2,3,4,5-tetrahydro-1H-3-benzazepin-7-yl)boronic acid (E264, Step 2), using the method of Example 264 Step 3; MS (ES+) m/e 322 [(M+H)—CO2tBu]+.