HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Bromomethyl)benzoic acid → Tert-butyl 4-(bromomethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Bromomethyl)benzoic acid | HCID 22599 | — |
| Reactant | tert-Butyl 4-iodobutanoate | HCID 12416448 | — |
| Solvent | Isobutylene | HCID 8255 | — |
| Product | Tert-butyl 4-(bromomethyl)benzoate | HCID 11414578 | — |
Reaction Steps
4-(Bromomethyl)benzoic acid (6 g, 26 mmol) and isobutene (30 ml) were reacted by the same procedure as described in Example 3 for the preparation of tert-butyl 4-iodobutanoate and afforded the title material (2.4 g) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06414179B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-f2cdec3ec7984235ab216d57a40052f4 |
| Source note | uspto-grants-2002_07 |