HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanide → HCID 54415491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | 2,6-Dimethyl-4-(1-phenyl-1H-pyrazol-3-yl)aminophenyl chloroacetate | HCID 49824850 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 54415491 | HCID 54415491 | — |
Reaction Steps
2,6-Dimethyl-4-(1-phenyl-1H-pyrazol-3-yl)aminophenyl chloroacetate, Example 4k, (1 g) and sodium cyanide (0.5 g) stirred in dimethyl sulfoxide for 16 hours gave, after dilution with brine, extraction with ethyl acetate and subsequent evaporation, the title compound (0.3 g), mp 116°-117° (from ethyl acetate/hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05428044 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-aea71330bab44cafb3bd1629fffe2846 |
| Source note | uspto-grants-1995_06 |