HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 2-(4-Bromophenyl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 131723369 | HCID 131723369 | — |
| Solvent | 2-Phenylethanol | HCID 6054 | — |
| Product | 2-(4-Bromophenyl)ethanol | HCID 72851 | — |
Reaction Steps
Hydroboration of 4-allyldimethylsilylphenethyl alcohol (1 Scheme 8) followed by Suzuki coupling reaction with the linker (2 Scheme 29) resulted in polymer-bound phenethyl alcohol compound (3 Scheme 29) which can be cleaved with bromine to give 4-bromophenethyl alcohol (4 Scheme 29).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06416861B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-a959eb06afea4e51a27ab0d8452ea9f5 |
| Source note | uspto-grants-2002_07 |