HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(tert-Butoxycarbonyl)-1,5-diaminopentane → HCID 18470602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(tert-Butoxycarbonyl)-1,5-diaminopentane | HCID 4352 | — |
| Reactant | 3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carbonyl chloride | HCID 2736581 | — |
| Product | HCID 18470602 | HCID 18470602 | 94.6% |
Reaction Steps
N-t-butyloxycarbonyl-1,5-diaminopentane (1.04 g, 5.14 mmol) and 3-(2-chloro-6-fluorophenyl)-5-methylisoxazol-4-oyl chloride (1.41 g, 5.14 mmol) were converted to 2.14 g of the title compound by the procedure of Preparation 1. (95%). MS(IS) m/z 412 (M+). IR(CHCl3) 3496, 3012, 2936, 1708, 1663, 1611, 1510 cm−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06417193B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-c5db2ec4526f489e87720bea3e1151eb |
| Source note | uspto-grants-2002_07 |