4-Ethoxybenzoyl Chloride → HCID 11794488, compound

HRID 2228583Notes

Reaction equation

HRID 2228583 reaction equation
[C:1]([C:3]1[CH:4]=[C:5]([CH:16]=[CH:17][CH:18]=1)[C:6]([NH:8][C:9]1[C:10]([NH2:15])=[CH:11][CH:12]=[CH:13][CH:14]=1)=[O:7])#[N:2].[CH2:19]([O:21][C:22]1[CH:30]=[CH:29][C:25]([C:26](Cl)=[O:27])=[CH:24][CH:23]=1)[CH3:20]>C(N(CC)CC)C>[C:1]([C:3]1[CH:4]=[C:5]([CH:16]=[CH:17][CH:18]=1)[C:6]([NH:8][C:9]1[C:10]([NH:15][C:26](=[O:27])[C:25]2[CH:24]=[CH:23][C:22]([O:21][CH2:19][CH3:20])=[CH:30][CH:29]=2)=[CH:11][CH:12]=[CH:13][CH:14]=1)=[O:7])#[N:2]

Participants

4

Reactant 2

HCID 1400594-Ethoxybenzoyl ChlorideHCID 10705025HCID 10705025, compound

Product 1

HCID 11794488HCID 11794488, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Using a procedure similar to 1B except starting with N1-(3-cyanobenzoyl)-1,2-benzenediamine, 4-ethoxybenzoyl chloride and triethylamine as base, the title compound was obtained as a white solid (39%); mp: 168-9° C.; IR(KBr): 1645, 1672, 2231, 3377 cm−1; MS(FD): 385(M+).

Sources & evidence

ORD record
ord-1eeca573f414434798e03c78121edd92
Source dataset
uspto-grants-2002_07
Patent number
US06417200B1

Reaction notes

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