HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 136383547, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Hydroxylamine HCl | HCID 21645 | — |
| Reactant | HCID 54272823 | HCID 54272823 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 136383547 | HCID 136383547 | 81.8% |
Reaction Steps
By the method of Example 4, 211.3 g of hydroxylammonium chloride in 400 ml of water and 240 g of pyridine were reacted with 342.4 g of 5-methylhex-5-ene-2,3-dione 3-(O-ethyloxime) in 800 ml of methanol. This gave 305 g of the title compound as a yellowish solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06417388B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-eab30ebbc5d2434cb2cc7fc7156cda7b |
| Source note | uspto-grants-2002_07 |