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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2228955Generated: November 2, 2026

Water → HCID 21685517, compound

https://huagongshe.com/reaction/2228955

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantBenzhydrylamineHCID 7036—
Reactant1,1'-CarbonyldiimidazoleHCID 68263—
SolventDichloromethaneHCID 6344—
ProductHCID 21685517HCID 21685517—

Reaction Steps

Benzhydrylamine (1.83 g) was dissolved in dichloromethane (3.0 ml). Carbonyldiimidazole (1.78 g) was added to the solution. The mixture was stirred at room temperature overnight. Water and dichloromethane were added thereto. The mixture was stirred, and then extracted with dichloromethane. The organic layer was dried over anhydrous magnesium sulfate. The solvent was then removed by distillation to give imidazole-1-carboxylic acid benzhydrylamide.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06417362B1
Source datasetuspto-grants-2002_07
ORD IDord-21520e7e4af04387a3f287e4e677ee5c
Source noteuspto-grants-2002_07