HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → 1-(2-Aminobenzoyl) 4-methylthiosemicarbazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | Benzoic acid, 2-amino-, hydrazide | HCID 94728 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-(2-Aminobenzoyl) 4-methylthiosemicarbazide | HCID 17810764 | — |
Reaction Steps
To a solution of 2-aminobenzoic hydrazide (1.5 g) in DMF was added 0.7 g of methyl isothiocyanate and the mixture was stand for a day. The solvent was removed and chloroform was added to the residue to give 2.1 of 1-(2-aminobenzoyl) 4-methylthiosemicarbazide as a precipitate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06420367B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-99869efab0564069b3594be42deab20d |
| Source note | uspto-grants-2002_07 |