Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2229231Generated: October 30, 2026

Sodium borohydride → HCID 18467036, compound

https://huagongshe.com/reaction/2229231

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium borohydrideHCID 4311764—
ReactantHCID 69945910HCID 69945910—
SolventMethanolHCID 887—
ProductHCID 18467036HCID 1846703672.3%

Reaction Steps

To a solution of (2-naphthyl) [2-(3-pyridyl)ethyl]ketone (2.14 g) in MeOH (40 ml) was added NaBH4 (0.34 g) and the mixture was stirred at room temperature for 30 minutes. After removal of the solvent, the residue was extracted with ethyl acetate. The extract was washed with water and brine, dried and concentrated to give the titled compound (1.56 g) as colorless prisms.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06420375B1
Source datasetuspto-grants-2002_07
ORD IDord-9366400d840048a886b56a15c0a19a4d
Source noteuspto-grants-2002_07