HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18467036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 69945910 | HCID 69945910 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18467036 | HCID 18467036 | 72.3% |
Reaction Steps
To a solution of (2-naphthyl) [2-(3-pyridyl)ethyl]ketone (2.14 g) in MeOH (40 ml) was added NaBH4 (0.34 g) and the mixture was stirred at room temperature for 30 minutes. After removal of the solvent, the residue was extracted with ethyl acetate. The extract was washed with water and brine, dried and concentrated to give the titled compound (1.56 g) as colorless prisms.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06420375B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-9366400d840048a886b56a15c0a19a4d |
| Source note | uspto-grants-2002_07 |