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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2229235Generated: October 31, 2026

Sodium borohydride → HCID 18467038, compound

https://huagongshe.com/reaction/2229235

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium borohydrideHCID 4311764—
ReactantHCID 18467031HCID 18467031—
SolventMethanolHCID 887—
ProductHCID 18467038HCID 1846703851.3%

Reaction Steps

To a solution of [2-(3-pyridyl)ethyl]-(5,6,7,8-tetrahydronaphthalen-2-yl)ketone (3.02 g) in MeOH (50 ml) was added NaBH4 (0.45 g) and the mixture was stirred at room temperature for 30 minutes. After removal of the solvent, the residue was extracted with ethyl acetate. The extract was washed with water and brine, dried and concentrated to give the titled compound (1.56 g) as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06420375B1
Source datasetuspto-grants-2002_07
ORD IDord-0372cfcb9a204a4b8026983318af1fb0
Source noteuspto-grants-2002_07