HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 1-benzofuran-2-carboxylate → 1-Benzofuran-2-Ylmethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 1-benzofuran-2-carboxylate | HCID 641368 | — |
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Product | 1-Benzofuran-2-Ylmethanol | HCID 2776263 | 79.2% |
Reaction Steps
The reaction of 2-ethoxycarbonylbenzofurane (27.40 g) with diisobutylaluminum hydride was carried out in the manner similar to that described in Reference Example 3 to give the titled compound (16.91 g) as a colorless oil. This compound was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06420375B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-edbf7a3e9d6e4484b4dd46671d59b14c |
| Source note | uspto-grants-2002_07 |