HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 1-(5-Fluoro-3-methyl-1-benzothiophen-2-yl)ethan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 5-Fluoro-3-methyl-benzo[b]thiophene | HCID 596828 | — |
| Product | 1-(5-Fluoro-3-methyl-1-benzothiophen-2-yl)ethan-1-one | HCID 18466998 | — |
Reaction Steps
The titled compound (7.43 g) was prepared as colorless crystals from 5-fluoro-3-methylbenzo[b]thiophene (9.97 g) and acetyl chloride (5.55 ml) by the similar reaction and purification procedure as described in Reference Example 35.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06420375B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-65998432506a42aba9a2dc5ae4cc508c |
| Source note | uspto-grants-2002_07 |