HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 11258008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | tert-Butyl piperazine-1-carboxylate | HCID 143452 | — |
| Reactant | 4-Phenoxyphenyl isocyanate | HCID 2734896 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11258008 | HCID 11258008 | 107.5% |
Reaction Steps
To a methylene chloride solution (25 mL) of N-tert-butoxycarbonylpiperazine (2.50 g, 13.4 mmol), 4-phenoxyphenyl isocyanate (2.83 mL, 13.4 mmol) was added, followed by stirring at room temperature overnight. Methanol was added to the reaction solution, and the solvent was evaporated to give the target compound (5.71 g, 14.4 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423716B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-d93d0a7e68354cbc98114b0bac1911ad |
| Source note | uspto-grants-2002_07 |