HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-3-methylbenzo(b)thiophene-2-sulfonyl chloride → HCID 18180122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-3-methylbenzo(b)thiophene-2-sulfonyl chloride | HCID 2735756 | — |
| Reactant | HCID 10881314 | HCID 10881314 | — |
| Product | HCID 18180122 | HCID 18180122 | — |
Reaction Steps
The title compound was prepared from 3-(2-dimethylaminoethoxy)-4iodoaniline (WO95/15954, Description 50) (109 mg, 0.36 mmol) and 5-chloro-3-methylbenzo[b]thiophene-2-sulfonyl chloride (100 mg, 0.36 mmol) using the method of Example 1 (70 mg, 36%) MH+=551/553.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423717B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-df6058ef2bc244a0a83e431bb53279cb |
| Source note | uspto-grants-2002_07 |