HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-3-methylbenzo(b)thiophene-2-sulfonyl chloride → HCID 18180163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-3-methylbenzo(b)thiophene-2-sulfonyl chloride | HCID 2735756 | — |
| Reactant | HCID 18180069 | HCID 18180069 | — |
| Product | HCID 18180163 | HCID 18180163 | — |
Reaction Steps
The title compound (E125) was prepared from 4-methoxy-2-methyl-3-(4-methylpiperazin-1-yl)phenylamine (D33) (58 mg, 0.247 mmol) and 5-chloro-3-methylbenzo[b]thiophene-2-sulfonyl chloride (70 mg, 0.247 mmol) using the method of Example 1 (103 mg, 81%). MH+=480/482.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423717B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-460181f2db5f4ad6a8d61d72ff8c24b4 |
| Source note | uspto-grants-2002_07 |