HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Bromobenzenesulfonyl chloride → HCID 18180189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Bromobenzenesulfonyl chloride | HCID 7396 | — |
| Reactant | HCID 18180121 | HCID 18180121 | — |
| Product | HCID 18180189 | HCID 18180189 | — |
Reaction Steps
The title compound (E129) was prepared from 4-methoxy-3-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)phenylamine (free base of D39) (107 mg; 0.49 mmol) and 4-bromobenzenesulfonylchloride (125 mg, 0.49 mmol) using the method of Example 1 (179 mg, 77%) MH+=437/439.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423717B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-71f50597f45f4dde8f03cb00e2bd1dc2 |
| Source note | uspto-grants-2002_07 |