HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18465469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18465425 | HCID 18465425 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18465469 | HCID 18465469 | 100% |
Reaction Steps
A mixture of t-butyl N-(2-{2-oxo-3-[1-(1-phenylcycloheptyl)-4-piperidyl]-2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate (35 mg, 0.0657 mmol, this was prepared as Preparation 18) and HCl solution in MeOH (2 ml) was stirred at room temperature for 15 h. The reaction mixture was concentrated in vacuo to give 33.2 mg (100%) of white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423725B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-f17cdd7fb8514f109a1d69855d55a91a |
| Source note | uspto-grants-2002_07 |