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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2230174Generated: October 30, 2026

Hydrochloric Acid → HCID 18465469, compound

https://huagongshe.com/reaction/2230174

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 18465425HCID 18465425—
SolventMethanolHCID 887—
ProductHCID 18465469HCID 18465469100%

Reaction Steps

A mixture of t-butyl N-(2-{2-oxo-3-[1-(1-phenylcycloheptyl)-4-piperidyl]-2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate (35 mg, 0.0657 mmol, this was prepared as Preparation 18) and HCl solution in MeOH (2 ml) was stirred at room temperature for 15 h. The reaction mixture was concentrated in vacuo to give 33.2 mg (100%) of white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06423725B1
Source datasetuspto-grants-2002_07
ORD IDord-f17cdd7fb8514f109a1d69855d55a91a
Source noteuspto-grants-2002_07