Ammonium Hydroxide → HCID 70179406, compound

Participants

Reaction Steps

The nitrile obtained in Step B (900 mg, 4.66.10−3 mol), diluted with methanol (30 ml), is hydrogenated with vigorous stirring at ambient temperature in the presence of ammonium hydroxide (2 ml) and Raney nickel. After 23 hours, the starting material has disappeared. After filtering over Celite, then rinsing and evaporating off the solvent under reduced pressure, the title amine is obtained in the form of an oil, which is used without being purified.

Provenance & Evidence