HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 15859298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 9817636 | HCID 9817636 | — |
| Product | HCID 15859298 | HCID 15859298 | — |
Reaction Steps
The compound obtained in Example 3 is reacted in the presence of NaH (1.5 eq) and dimethyl sulphate (1.2 eq). The reaction is monitored using TLC. When all the starting material has disappeared, the reaction mixture is hydrolysed and then extracted. After evaporating off the solvents, the title product is isolated by flash chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423870B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-973d7bebbda442fdae8734a466655bab |
| Source note | uspto-grants-2002_07 |