HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18466109, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 18466228 | HCID 18466228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18466109 | HCID 18466109 | — |
Reaction Steps
The compound of Example 27, dissolved in dichloromethane, is added dropwise at 0° C. to a suspension of aluminium chloride and benzylthiol. The reaction is monitored by TLC. When the reaction has ended, the reaction mixture is poured onto ice and then acidified using 1N HCl. Customary extraction is carried out and the title compound is isolated by chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423870B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-5cb81d3c76644eafad51463530e80a4b |
| Source note | uspto-grants-2002_07 |