HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 66756432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | (3S)-2-Oxo-3-tert-butoxycarbonylamino-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine-1-acetic acid methyl ester | HCID 54305289 | — |
| Product | HCID 66756432 | HCID 66756432 | — |
Reaction Steps
(600a/103, 4.0 g, 11.4 mmol) in 20 ml of CH2Cl2 for 20 min then stirred for 1 h at RT. The reaction was evaporated to give (3S)-2-oxo-3-amino-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine-1-acetic acid methyl ester hydrochloride as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06423840B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-443f277eef3e446ebc3b0dcc90767250 |
| Source note | uspto-grants-2002_07 |