HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 18463711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 1-(Chloromethyl)-4-methanesulfonylbenzene | HCID 123530 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 18463711 | HCID 18463711 | — |
Reaction Steps
4-(Methylsulfonyl)benzyl chloride (Transworld Chemical) (121 mmol, 24.7 g) and triphenylphosphine (130 mmol, 34.1 g) were heated at reflux in toluene (125 ml) with stirring for 56 hours. The reaction was cooled, and the title compound was collect by filtration (48.0 g, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06426360B1 |
| Source dataset | uspto-grants-2002_07 |
| ORD ID | ord-542d0617018c40eba1f2e177e1119482 |
| Source note | uspto-grants-2002_07 |