Water → HCID 86742502, compound

HRID 2231149Notes

Reaction equation

HRID 2231149 reaction equation
[CH2:1]([O:3][CH:4]([O:6][CH:7]([CH3:11])[C:8]([O-:10])=[O:9])[CH3:5])[CH3:2].[K+].O.[Cl-].[Ca+2:15].[Cl-]>>[CH2:1]([O:3][CH:4]([O:6][CH:7]([CH3:11])[C:8]([O-:10])=[O:9])[CH3:5])[CH3:2].[Ca+2:15].[CH2:1]([O:3][CH:4]([O:6][CH:7]([CH3:11])[C:8]([O-:10])=[O:9])[CH3:5])[CH3:2]

Participants

4

Reactant 3

HCID 962WaterHCID 5284359Calcium ChlorideHCID 23720076100743-68-8

Product 1

HCID 86742502HCID 86742502, compoundYield 39.7%

Procedure

To a 50 mL flask containing 5.9 g (0.05 mole) product of Example 1 and 6.5 g (0.36 mole) water at 20° C. is added 20 g 50% calcium chloride aqueous solution. A white crystalline solid material was isolated by filtration and dried yielding 3.6 g (20%) calcium 2-[(1'-ethoxy)ethoxy]propanoate.

Workup

  1. customA white crystalline solid material was isolated by filtration
  2. customdried

Sources & evidence

ORD record
ord-a07ba101d7594dfb8e82e5d8544d5bd0
Source dataset
uspto-grants-1988_11
Patent number
US04781762

Reaction notes

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