HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21286356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 21286361 | HCID 21286361 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 21286356 | HCID 21286356 | 102.1% |
Reaction Steps
Methyl iodide (1.08 g) was added dropwise to a solution of 3-dimethylaminomethyl-8-(2-methoxybenzyloxy)2-methylimidazo[1,2-a]pyridine (3.42 g) in acetone (34 ml) and chloroform (10 ml) at room temperature and the mixture was stirred for 24 hours. The resulting precipitate was collected by filtration, washed with acetone, and dried in a desiccator to give 8-(2-methoxybenzyloxy)-2-methyl-3-trimethylammoniomethylimidazo[1,2-a]pyridine iodide (3.63 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782055 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-985a1e89a6ee4d6eaf0135a20119598f |
| Source note | uspto-grants-1988_11 |