HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N,N,N'-triphenyl-N'-4-pyridinylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N,N-Diphenylcarbamic chloride | HCID 65741 | — |
| Reactant | N-phenylpyridin-4-amine | HCID 89945 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | N,N,N'-triphenyl-N'-4-pyridinylurea | HCID 14302814 | — |
Reaction Steps
A solution of 8.51 g (0.05 mol) of N-phenyl-4-pyridinamine in 400 ml of chloroform is mixed with 11.5 g (0.11 mol) of triethylamine. To this mixture is added, dropwise with stirring, a solution of 11.6 G (0.05 mol) of diphenylcarbamic chloride in chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04782071 |
| Source dataset | uspto-grants-1988_11 |
| ORD ID | ord-e89a5c769b7a4fa2a44cf30d19b26566 |
| Source note | uspto-grants-1988_11 |