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HRID2231231

反应详情

EQUATION

反应方程式

HRID 2231231 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(Cl)N(c1ccccc1)c1ccccc1
HCID65741

Diphenylcarbamyl chloride

C13H10ClNO

结构：c1ccc(Nc2ccncc2)cc1
HCID89945

N-Phenylpyridin-4-amine

C11H10N2

PRODUCTS

生成物

1
结构：O=C(N(c1ccccc1)c1ccccc1)N(c1ccccc1)c1ccncc1
HCID14302814

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClC(Cl)Cl
溶剂HCID6212

Chloroform

CHCl3

2 次

PROCEDURE

实验过程

A solution of 8.51 g (0.05 mol) of N-phenyl-4-pyridinamine in 400 ml of chloroform is mixed with 11.5 g (0.11 mol) of triethylamine. To this mixture is added, dropwise with stirring, a solution of 11.6 G (0.05 mol) of diphenylcarbamic chloride in chloroform.

WORKUP

后处理

  1. additionTo this mixture is added